弹性力学的复变量无网格局部 Petrov-Galerkin 法

复变量移动最小二乘法构造形函数, 其优点是采用一维基函数建立二维问题的试函数, 使得试函数中所含的待定系数减少, 从而有效提高计算效率. 文章基于复变量移动最小二乘法和局部Petrov-Galerkin弱形式, 采用罚函数法施加边界条件, 推导相应的离散方程, 提出弹性力学的复变量无网格局部Petrov-Galerkin法. 数值算例验证了该方法的有效性.     

混沌超宽带信号的光学产生及其链路传输

用光反馈半导体激光器产生混沌超宽带(UWB)信号, 搭建了混沌UWB光载无线通信链路, 实现了360, 720 Mbit/s和1.44 Gbit/s三种不同传输速率下混沌UWB脉冲信号的生成和传输. 在未经任何色散补偿处理的情况下, 1.44 Gbit/s的混沌UWB信号在经过10 km单模光纤和0.6 m无线链路传输后, 在天线接收端被成功解调. 由于混沌UWB信号输出的随机性, 对应的UWB信号频谱中未出现任何离散的谱线. 这意味着利用混沌UWB信号实现的光载无线通信链路, 可以完全避免离散谱线对系统传输性能的劣化.     

复合应力下泡沫铝屈服行为实验研究

 采用ARCAN双轴加载装置和材料实验机（INSTRON 5544）,对相对密度为8.5%的闭孔泡沫铝（Alporas）进行了不同应变率下的双轴加载实验。在宏观等效应变率为7.0×10^-3~1.0×10^-1 s^-1范围内测得实验屈服面,并与泡沫金属的3种屈服准则进行了比较。比较结果表明：在主应力空间下,实验屈服面与Miller和Deshpande-Fleck屈服准则吻合较好,Gibson屈服准则过小估计了测试泡沫铝的实验屈服面;被测泡沫铝的实验屈服面在宏观等效应变率7.0×10^-3~1.0×10^-1 s^-1范围内对应变率不敏感。     

以双(2-二苯基磷苯基)醚为配体的蓝色磷光铜(Ⅰ) 配合物的合成及光电特性研究

合成了一种新型的室温天蓝色磷光发射材料双(2-二苯基磷苯基)醚碘合铜(Ⅰ)([(POP)CuI]₂)配合物。通过红外光谱、X-射线单晶衍射确定其分子结构,并对其光电特性进行了详细研究。结果表明:[(POP)CuI]₂为二聚体结构,主要吸收峰为227,268,291 nm,最大发射峰为475 nm,光学带隙为2.93 eV。以[(POP)CuI]₂作为客体掺杂在主体CBP中作为发光层,制备了结构为ITO/NPB(30 nm)/CBP∶[(POP)CuⅠ]₂(30 nm,8%)/BAlq(10 nm)/Alq₃ (30 nm)/LiF(1 nm)/Al(200 nm)的器件,其电致发光峰为476 nm,最大亮度为9 539 cd/m²,最大电流效率为1.9 cd/A。     

高效液相色谱法快速测定化妆品中的防腐剂

建立了化妆品中4种4-羟基苯甲酸酯类防腐剂HPLC的快速测定新方法,该方法采用自制的C18柱(4.6mm×250mm,5μm)为分离柱,以甲醇-水(70∶30,V/V)为流动相,检测波长为254nm。结果表明,该检测方法比《化妆品卫生规范》(2007版)更简单,检出限远低于规范中的限量,达到0.0001—0.0003μg,而且实现了4种4-羟基苯甲酸酯类防腐剂的快速分离,4种防腐剂在10—300μg/mL范围内呈良好线性关系(r≥0.9998),平均回收率为98.7%—111.9%,相对标准偏差为0.19%—0.79%。方法操作简单,分析速度快、灵敏度高,适合日常化妆品防腐剂的快速分析测定。     

Additive maps preserving rank-one operators on nest algebras

In this article, we give a thorough discussion of additive maps between nest algebras acting on Banach spaces which preserve rank-one operators in both directions.     

Encrypting image by assembling the fractal-image addition method and the binary encoding method

The fractal-image addition method and the binary encoding method are assembled to form a hybrid method for encrypting a digital covert image. For this hybrid method, a host image is used to create an overt image with the information of the covert image. First, the fractal-image addition method is used to add some fractal images and the covert image to form an image-mixing matrix. Then, all the pixel values of the image-mixing matrix are transferred into binary data. Finally, the binary data are encoded into the host image to create an overt image. The pixels of the overt image contain eight groups of codes used for reconstructing the covert image. The eight groups of codes are identification codes, row amount codes, covert-image dimension codes, fractal-image amount codes, starting-pixel codes, character amount codes, character codes, and information codes. The overt image and the host image look almost the same for eyes. Furthermore, the covert image can be directly reconstructed from the overt image without using the host image. The most important feature is that the reconstructed covert image is identical to the original covert image, i.e. there is no distortion in the decoding work.     

Fundamental and harmonic mode-locking in erbium-doped fiber laser based on graphene saturable absorber

Graphene-based passively mode-locked erbium doped fiber laser is presented. Multilayer graphene was obtained by mechanical exfoliation of pure graphitic block and deposited on the fiber ferrule. The mode-locking performance was investigated under various laser pumping conditions. The laser could operate at fundamental repetition rate of 16.34 MHz with 844 fs pulse duration and 30 mW average output power. Also harmonic-mode locking of the laser is demonstrated. 294 and 800 MHz repetition rates were obtained (corresponding to the 18th and 49th harmonic of the fundamental repetition frequency, respectively) with nearly transform-limited pulses.     

Novel layered calcosilicate-immobilized iron-based diimine catalyst for ethylene polymerization

A novel layered calcosilicate (CAS-1) was employed to immobilize an iron-based diimine catalyst 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron chloride (I) onto it to form a supported catalyst (CC) for the first time. The crystal structure of CAS-1 was determined by X-ray crystallographic analysis in addition to SEM characterization. The CC-catalyzed ethylene polymerization exhibited good catalytic activities with either co-catalyst methylaluminoxane (MAO) or triethylaluminum (TEA). The resulting polyethylenes possessed not only higher molecular weight, melting temperature (T_m), and decomposition onset temperature (T_onset) than those obtained with its homogeneous counterpart, but also a unique morphology.     

Aspects of thermal martensite in a FeNiMnCo alloy

Thermal martensite characteristics in Fe–29%Ni–2%Mn–2%Co alloy were investigated with scanning electron microscopy (SEM) and Mössbauer spectroscopy characterization techniques. SEM observations obviously revealed the lath martensite morphology in the prior austenite phase of examined alloy. As well, the martensitic transformation kinetics was found to be as athermal type. On the other hand, Mössbauer spectroscopy offered the paramagnetic austenite phase and ferromagnetic martensite phase with their volume fractions. Also, the internal magnetic field of the martensite was measured as 32.9 T from the Mössbauer spectrometer.